The CAMSIZER 3D particle analyzer combines all the advantages of dynamic image analysis (ISO 13322-2) in a completely redesigned measuring system, setting new standards in the characterization of bulk solids.
Unique 3D Analysis: Thanks to the extended field of view and long drop distance, each particle is analyzed up to 30 times and in different orientations, making the actual, three-dimensional particle morphology accessible for analysis. The evaluation of the “3D tracks” also provides much more meaningful shape analysis than ever before.
Proven 2-Camera System: The new ZOOM camera inside the CAMSIZER 3D (9 MPx) allows for the evaluation of fine particles with great accuracy. In combination with the BASIC camera (5 Mpx), this enables a wide measuring range from 20 µm to 30 mm. CAMSIZER 3D is the first choice for the analysis of dry, free-flowing bulk solids in both quality control and for research applications.
The CAMSIZER 3D utilizes a funnel, vibrating feed chute, LED strobe backlighting, powerful high-speed cameras, and sophisticated software to perform the measurements.
The particles travel down the vibrating feeder and fall into the sensing zone, creating a tumbling motion as they fall. The CAMSIZER software tracks each particle as it passes between light source and cameras, taking up to 250 images per second. As the particle is tracked, multiple images are recorded, measuring length, width, thickness, perimeter, area and various shape descriptors. The software automatically aligns the images for viewing, with up to 30 images per particle. This creates a “particle track”, a sequence of images of the same particle in different orientations. From this, distributions can be calculated, based on one or more size or shape parameters. Filters can be applied to isolate groups of particles of particular interest for more targeted analysis.
In the particle track, the software determines the width and the length of each particle projection:
In contrast, traditional 2D analysis captures only one image per particle in random orientation, even if the particle in measured multiple times at increased acquisition rate, there is no “mapping” of one image to another. Each individual image is treated as a new, independent measurement event. The true length, width, thickness, and shape is obscured by this. Rather, the “length” measured in 2D mode is a mixture between true 3D length and true 3D width; the “width” measured in 2D mode is a mixture between true 3D width and true 3D thickness. Only if the particles can be mechanically aligned, meaningful results are obtained in 2D mode. In the past, however, this was only feasible for some special particle shapes like cylinders.
Measurement in 2D Mode
Measurement in 3D Mode
Microtrac’s unique dual camera technology is a landmark in the development of Dynamic Image Analysis. By simultaneously employing two cameras with different magnifications, extremely wide dynamic measuring ranges are achieved. This is accomplished without hardware adjustments or modifications and without compromising the accuracy.
Each camera is specialized for one size range. The ZOOM camera analyzes fine particles with highest resolution whereas the BASIC camera detects the larger particles with excellent statistics. A special algorithm combines the information provided by both cameras, covering a size range of more than three orders of magnitude.
This arrangement resolves a significant drawback of many image analysis systems that employ only one camera, e. g. microscopes. Such instruments either cannot correctly report the fine particles in wide size distributions, or the large particles are not captured reliably due to the small field of view.
Compared to previous CAMSIZER models the CAMSIZER 3D features a significantly higher camera resolution and frame rate by employing a ZOOM camera with 9 megapixels and a BASIC camera with 5 megapixels at a frame rate of up to 250 fps.
This allows superior image quality and particle detection, for all coarse and fine samples. Broad and narrow distributions are measured with the same accuracy and precision.
The image width of the ZOOM camera is the same as that of the BASIC camera, which ensures excellent reproducibility of the measurement results within a short measurement time.
Традиционно ситовой анализ является стандартом для анализа качества продуктов во взаимоотношениях между поставщиком и покупателем. Быстрой и достаточно эффективной альтернативой ситовому анализу - метод должен представлять результаты измерения, которые были бы полностью сопоставимы с результатами рассева.
Для этих целей программное обеспечение анализатора CAMSIZER включает в себя алгоритм имитирующий результаты рассева.
Вот почему многие пользователи уже успешно заменили трудоемкий ситовой анализ на анализатор CAMSIZER безо всяких потерь и сожалений. Автоматическое, не требующее дополнительных усилий измерение позволяет получать более надежные и воспроизводимые результаты.
Превосходная сопоставимость результатов измерения на ситах и анализаторе CAMSIZER образцов гранулированных удобрений
Microtrac предлагает различные наборы загрузочных воронок и лотков для конкретных применений. С помощью загрузочных направляющих подачи поток образцов может быть ориентирован таким образом, что, например, длинные частицы, такие как экструдаты, всегда измеряются в правильной ориентации. Различные виды делителей образцов обеспечивают репрезентативный отбор образцов порошков, гранул и многих других типов сыпучих материалов перед анализом.
Calibration Reticle
A certified reference object is available for the CAMSIZER 3D, which allows the user to calibrate the device in a few seconds. This object is a glass pane that is inserted precisely into the measuring zone. Circles of various sizes are lithographically applied to the calibration reticle. The reproduction scale of the cameras is determined by measuring the circles. After completion of the calibration process, a protocol can be printed to document the proper condition of the CAMSIZER 3D.
Feeder and Funnel Kits
Different chutes and funnel sets are available for the CAMSIZER 3D, which are suitable for different sample volumes and particle size ranges. In 3D mode, the width of the feeder has an influence on the number of particle images in the 3D tracks, as narrower chutes enable a higher acquisition rate due to the reduced image size. However, the use of narrow chute increases the measurement time. MICROTRAC will be happy to advise you on the selection of the most suitable configuration for your application.
Guidance Sheets
The guidance sheet channels the sample flow before it enters the measurement zone. This can be advantageous, for example, when particles jump on the feeder. The long shield prevents the particles from being hurled over the measuring shaft and directs them into the focal plane. The guidance sheet also provides protection from air currents that could cause unwanted turbulence in the measurement zone.
Audit Trail Manager
The Audit Trail Manager is a software package that enables operation in accordance with the specifications of the 21 CFR part 11. This standard is particularly relevant in the pharmaceutical industry and its suppliers. The program option offers extensive user administration with various access levels and logs all processes in an encrypted database, the Audit Trail. Measurement results can be electronically signed for quality assurance.
Sample Splitters
Every measurement is only as good as the sampling and sample preparation that preceded it. Especially in the case of flowable bulk materials with a wide size distribution, segregation occurs, which leads to an incorrect distribution of particle sizes in the sample aliquot. By using a sample divider, representative partial samples can be generated in a simple way, which guarantee a meaningful result. MICROTRAC strongly recommends corrugated dividers and rotary sample dividers from RETSCH, also part of the Verder Scientific Group.
The Autosampler is a fully automatic sample feeding system for the CAMSIZER 3D which can be easily retrofitted to existing instruments.
It processes up to 14 samples (extendable to 40 samples or more) in a row without the need for the operator’s intervention. The correct measurement settings can be read from the barcodes on the sample beaker. The Autosampler is suitable for continuous operation and allows effortlessly measuring more than 150 samples per day, even by untrained operators.
Typical applications for the CAMSIZER 3D Autosampler system include sand, superabsorbent polymers, rice, coke, tea, rubber granules, EPS, sugar, glass beads, salt, and many more.
Многие свойства сыпучих материалов, такие как текучесть, растворимость, эффективность фильтрации, реакционная способность, абразивность и вкус, значительно зависят от размера частиц. Поэтому определение размера частиц обычно используется как часть контроля качества во многих различных отраслях промышленности.
Especially when products with specific geometry are produced, such as extrudates, abrasives, pharmaceutical pellets or fertilizer granules, shape analysis with the CAMSIZER 3D provides important measurement data determining the quality of the sample within a few minutes. Another advantage is that the method can be largely automated via automatic sample feeding systems or online connection.
песок
фармацевтические препараты
сахар
With the patented 3D particle measurement, the length distribution of extrudates can be determined accurately. A rod-shaped ceramic extrudate with a length of 6-8 mm was measured in 3D mode, in 2D mode and with a caliper. The result shows that the 3D length corresponds to the result of the caliper, but the 2D length gives a distribution that is “too short”. Thus, the 3D image analysis is as accurate as the caliper measurement but characterizes a significantly larger number of particles in a fraction of the time.
Particle size and shape are important parameters for the quality of fertilizers. During the granulation process the pellets will be shaped as nearly spherical particles. A non-optimal process will first be recognized by a change in particle shape as the granulate will be ellipsoidal rather than spherical. The diameter will stay the same and it will not be reported in the standard sieve analysis. By measuring the roundness and aspect ratio the CAMSIZER 3D will detect even the smallest changes in product quality.
Top: Non-spherical fertilizer pellet showing true shape on several images of the track, but also some circular projections.
Bottom: Spherical fertilizer pellets: Circular projection on every image of the 3D track.
Many natural or man-made particles have three clearly distinguishable main axes. These include extrudates, pellets, or even almonds and coffee beans. The example shows the comparison of the length, width, and thickness measurement of a sample of coffee beans. For each size definition, the correct distribution is displayed. In comparison, the 2D length measurement is “too short” and the 2D width measurement is a mixture of the true thickness and true width. Consequently, the true thickness / length ratio of the 3D measurement is smaller and more narrowly distributed than the aspect ratio in the 2D analysis.
Particle size distribution of a sample of coffee beans:
2D width (grey), 2D length (grey), 3D thickness (green), 3D width (red), 3D length (blue)
Superabsorbent polymers can absorb large amounts of a liquid relative to their own mass. They are used in granular form, for example in baby diapers as a drying agent. Particle size is an essential quality criterion with a distribution that is usually between 100 µm and 1000 µm. Small particle size equals high specific surface area, hence faster liquid absorption. The specifications are typically based on classic sieve analyses. The CAMSIZER 3D delivers 100 % equivalent results and can fully replace this established but time-consuming and error-prone technique.
Glass beads are used, for example, in road markings to ensure traffic safety using high retro-reflectivity beads . Fused or deformed beads reduce the reflectivity, thus harming the product quality. The CAMSIZER 3D can measure the percentage of defective beads with better accuracy than conventional 2D detection because 2D only measures one random orientation, in which the true morphology of the particle can be obscured. The graph shows the distribution of the aspect ratio of a glass sample in 2D mode and in 3D mode. In the 3D measurement, more elongated particles are detected because each glass bead is examined from different angles which leads to a difference of 17% in this case.
The 3D track shows two fused beads with an aspect ratio between 0.82 and 0.35 depending on the orientation. 3D analysis detects the true shape of particles from multiple projections and allows more accurate shape analysis.
The CAMSIZER 3D is ideally suited to characterize the growth of granules and pellets, i.e. in a granulation process. The results provide information about the thickness and homogeneity of coatings, dust fractions or oversized particles (agglomerates). This information is the basis for the prediction of such complex parameters as the release rate of an active pharmaceutical ingredient (API) from the granule in the human body. The example shows the initial material (green) and four coating steps (two repeated measurements for each). Even the last process step with a coating thickness of only 2.5 µm is reliably detected thanks to the extremely high reproducibility.
Чтобы найти лучшее решение для вашего применения в определении размера частиц, посетите нашу базу данных применений
All parameters at a glance: Dynamic Digital Image Analysis provides a wealth of information about the sample material at hand. The powerful DIMENSIONS software records dozens of parameters on each individual particle and presents the results in a clear, standard-compliant measurement report that can be adapted to individual needs.
Our instruments are recognized as the benchmark tools for a wide range of application fields in science and research. This is reflected by the extensive citations in scientific publications. Feel free to download and share the articles provided below.
| Принцип измерения | 2D and 3D Dynamic Image Analysis according to ISO 13322-2 |
| Диапазон измерения | recommended range 20 μm to 30 mm (with no hardware adjustment) |
| Параметры | particle size, shape, volume, density, transparency and number |
| Камера | Dual Camera Technology, 9 MP + 5 MP; up to 250 images per second |
| Время анализа | approx. 2 to 5 min (depends on required measurement statistics) |
| Программное обеспечение | Microtrac DIMENSIONS |
| Размеры | 850 × 650 × 350 мм |
| Вес | прибл. 40 кг |
| CE сертифицирован | Да |
| Подача сжатого воздуха | 6 to 8 bar |
| Расход сжатого воздуха | макс. 10 л/мин |
| Размеры | прибл. 1450 x 900 x 490 мм |
| Вес | прибл. 60 кг |
| Образец корма | 14 samples can be placed on the conveyor belt simultaneously (opt. up to 40 samples); continuous (and unattended) operation possible; sample feed by electro-pneumatic robot arm; emergency stop-button |
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